| Bruker X8 Proteum diffractometer | 2448 independent reflections |
| Radiation source: fine-focus rotating anode | 2196 reflections with I > 2σ(I) |
| graded multilayer optics | Rint = 0.041 |
| Detector resolution: 5.6 pixels mm-1 | θmax = 68.5°, θmin = 4.8° |
| φ and ω scans | h = −17→17 |
| Absorption correction: multi-scan (SADABS in APEX2; Bruker, 2006) | k = −13→13 |
| Tmin = 0.805, Tmax = 0.979 | l = −17→21 |
| 19606 measured reflections |
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