Table 1. Hydrogen-bond geometry (Å, °).
D—H⋯A | D—H | H⋯A | D⋯A | D—H⋯A |
---|---|---|---|---|
O1—H1A⋯O7 | 0.84 | 2.36 | 3.065 (3) | 142 |
O2—H2A⋯O45i | 0.84 | 2.00 | 2.809 (3) | 161 |
O2—H2A⋯O45′i | 0.84 | 1.95 | 2.633 (11) | 138 |
O5—H5A⋯O47 | 0.84 | 1.76 | 2.578 (15) | 163 |
O5—H5A⋯O45ii | 0.84 | 2.46 | 3.024 (4) | 125 |
O5′—H5′⋯O45ii | 0.84 | 1.66 | 2.47 (3) | 163 |
O5′—H5′⋯O45′ii | 0.84 | 2.40 | 3.20 (3) | 159 |
O6—H6C⋯O12 | 0.84 | 2.04 | 2.845 (2) | 161 |
O6—H6C⋯O13 | 0.84 | 2.31 | 2.742 (2) | 112 |
O7—H7A⋯O26i | 0.84 | 2.14 | 2.956 (3) | 165 |
O11—H11A⋯O40 | 0.84 | 1.78 | 2.595 (2) | 163 |
O12—H12C⋯O31iii | 0.84 | 1.85 | 2.676 (2) | 167 |
O15—H15A⋯O41iv | 0.84 | 2.04 | 2.870 (3) | 172 |
O16—H16A⋯O38v | 0.84 | 1.90 | 2.733 (3) | 174 |
O17—H17A⋯O11 | 0.84 | 2.06 | 2.889 (2) | 171 |
O20—H20A⋯O43 | 0.84 | 1.93 | 2.725 (3) | 157 |
O20—H20A⋯O50 | 0.84 | 2.12 | 2.80 (3) | 138 |
O21—H21A⋯O27 | 0.84 | 1.99 | 2.810 (2) | 167 |
O21—H21A⋯O28 | 0.84 | 2.36 | 2.794 (2) | 112 |
O22—H22A⋯O16 | 0.84 | 1.97 | 2.776 (2) | 160 |
O22—H22A⋯O23 | 0.84 | 2.41 | 2.821 (2) | 111 |
O25—H25A⋯O39vi | 0.84 | 1.90 | 2.743 (3) | 178 |
O26—H26A⋯O37iii | 0.84 | 1.83 | 2.668 (3) | 176 |
O27—H27A⋯O5v | 0.84 | 2.09 | 2.821 (3) | 145 |
O30—H30C⋯O15vii | 0.84 | 2.06 | 2.858 (3) | 158 |
O30—H30C⋯O14vii | 0.84 | 2.37 | 2.945 (2) | 126 |
O31—H31A⋯O2 | 0.84 | 2.01 | 2.844 (2) | 172 |
O32—H32A⋯O26 | 0.84 | 2.04 | 2.871 (2) | 170 |
O35—H35A⋯O37i | 0.84 | 2.08 | 2.890 (2) | 161 |
O36—H36⋯O11ii | 0.84 | 2.02 | 2.854 (2) | 173 |
O37—H37A⋯O6 | 0.824 (17) | 2.05 (2) | 2.837 (2) | 160 (3) |
O37—H37B⋯O32viii | 0.849 (17) | 1.910 (18) | 2.753 (2) | 171 (3) |
O38—H38A⋯O20 | 0.828 (17) | 2.11 (2) | 2.865 (3) | 152 (3) |
O38—H38B⋯O30ix | 0.817 (17) | 1.857 (18) | 2.672 (3) | 176 (3) |
O39—H39A⋯O22ii | 0.856 (18) | 1.898 (18) | 2.749 (3) | 173 (3) |
O39—H39B⋯O38 | 0.861 (18) | 2.18 (2) | 2.959 (3) | 151 (3) |
O40—H40A⋯O41x | 0.879 (18) | 2.21 (3) | 2.787 (3) | 123 (3) |
O40—H40B⋯O35xi | 0.869 (18) | 1.91 (2) | 2.770 (3) | 168 (3) |
O41—H41A⋯O20 | 0.844 (17) | 2.134 (18) | 2.976 (3) | 175 (3) |
O41—H41A⋯O19 | 0.844 (17) | 2.63 (3) | 3.048 (2) | 112 (3) |
O41—H41B⋯O25 | 0.840 (18) | 1.95 (2) | 2.769 (3) | 166 (3) |
O42—H42C⋯O21ii | 0.852 (18) | 2.09 (2) | 2.932 (3) | 173 (3) |
O42—H42D⋯O48 | 0.805 (18) | 1.90 (4) | 2.53 (3) | 135 (3) |
O42—H42D⋯O39 | 0.805 (18) | 2.34 (3) | 3.038 (3) | 146 (3) |
Symmetry codes: (i) ; (ii) ; (iii) ; (iv) ; (v) ; (vi) ; (vii) ; (viii) ; (ix) ; (x) ; (xi) .