Table 1. Hydrogen-bond geometry (Å, °).
| D—H⋯A | D—H | H⋯A | D⋯A | D—H⋯A |
|---|---|---|---|---|
| N1—H1NB⋯O12i | 0.92 | 2.47 | 3.228 (12) | 140 |
| N1—H1NB⋯O16i | 0.92 | 2.51 | 3.059 (11) | 119 |
| N1—H1NB⋯O18i | 0.92 | 2.49 | 3.132 (12) | 128 |
| N1—H1NB⋯O22i | 0.92 | 2.28 | 3.016 (11) | 136 |
| O1S—H1O⋯O38ii | 0.72 | 2.18 | 2.669 (11) | 126 |
| N1—H1NA⋯O2S | 0.92 | 2.24 | 2.725 (12) | 112 |
| N1—H1NA⋯O36iii | 0.92 | 2.01 | 2.855 (12) | 152 |
| N2—H2NB⋯O3S | 0.92 | 2.18 | 2.687 (12) | 114 |
| N2—H2NB⋯O40iv | 0.92 | 1.93 | 2.744 (11) | 146 |
| N2—H2NA⋯O6v | 0.92 | 1.90 | 2.810 (11) | 170 |
| O4S—H4O⋯O3W | 0.92 | 1.73 | 2.647 (12) | 170 |
| N3—H3NB⋯O3S ii | 0.92 | 2.18 | 2.909 (13) | 135 |
| N3—H3NA⋯O5S | 0.92 | 2.16 | 2.672 (11) | 114 |
| N3—H3NA⋯O10S | 0.92 | 2.05 | 2.856 (12) | 145 |
| O6S—H6O⋯O1W | 0.84 | 1.88 | 2.638 (13) | 149 |
| N4—H4NB⋯O7 | 0.92 | 1.96 | 2.821 (13) | 155 |
| O7S—H7O⋯O21vi | 0.84 | 1.87 | 2.689 (11) | 165 |
| N4—H4NA⋯O8S | 0.92 | 2.29 | 2.701 (13) | 107 |
| N5—H5NB⋯O10S | 0.92 | 2.26 | 2.709 (12) | 109 |
| N5—H5NB⋯O25i | 0.92 | 2.20 | 3.005 (11) | 146 |
| O9S—H9O⋯O2W | 0.89 | 1.86 | 2.651 (12) | 147 |
| N5—H5NA⋯O31 | 0.92 | 2.25 | 2.830 (12) | 120 |
| N5—H5NA⋯O8S vii | 0.92 | 2.00 | 2.855 (13) | 154 |
Symmetry codes: (i)
; (ii)
; (iii)
; (iv)
; (v)
; (vi)
; (vii)
.