| Rigaku Saturn diffractometer | 2798 independent reflections |
| Radiation source: rotating anode | 2631 reflections with I > 2σ(I) |
| confocal | Rint = 0.040 |
| Detector resolution: 14.63 pixels mm-1 | θmax = 27.9°, θmin = 2.3° |
| ω scans | h = −9→9 |
| Absorption correction: multi-scan (CrystalClear; Rigaku, 2005) | k = −19→20 |
| Tmin = 0.899, Tmax = 0.967 | l = −14→14 |
| 14476 measured reflections |
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