| Bruker Kappa Duo APEXII diffractometer | 3561 independent reflections |
| Radiation source: fine-focus sealed tube | 3536 reflections with I > 2σ(I) |
| graphite | Rint = 0.012 |
| 0.5° φ scans and ω scans | θmax = 68.9°, θmin = 4.3° |
| Absorption correction: multi-scan (SADABS; Sheldrick, 1997) | h = −6→7 |
| Tmin = 0.692, Tmax = 0.753 | k = −10→10 |
| 7546 measured reflections | l = −13→13 |