| Stoe IPDSII two-circle diffractometer | 2360 reflections with I > 2σ(I) |
| Radiation source: fine-focus sealed tube | Rint = 0.062 |
| graphite | θmax = 25.6°, θmin = 3.4° |
| ω scans | h = −28→23 |
| 6868 measured reflections | k = −5→6 |
| 2823 independent reflections | l = −15→15 |
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