| Oxford Diffraction Xcalibur Ruby Gemini diffractometer | 4191 independent reflections |
| graphite | 3514 reflections with I > 2σ(I) |
| Detector resolution: 10.434 pixels mm-1 | Rint = 0.029 |
| ω scans | θmax = 25.7°, θmin = 2.3° |
| Absorption correction: analytical (CrysAlis PRO; Oxford Diffraction, 2009) | h = −16→16 |
| Tmin = 0.836, Tmax = 0.892 | k = −17→17 |
| 61823 measured reflections | l = −27→27 |