Oxford Diffraction Xcalibur (Sapphire2, large Be window) diffractometer | 1761 independent reflections |
Radiation source: Enhance (Mo) X-ray Source | 1448 reflections with I > 2σ(I) |
graphite | Rint = 0.022 |
Detector resolution: 8.1929 pixels mm-1 | θmax = 26.8°, θmin = 2.3° |
ω–scan | h = −8→6 |
Absorption correction: multi-scan (CrysAlis PRO; Oxford Diffraction, 2009) | k = −3→4 |
Tmin = 0.678, Tmax = 0.944 | l = −31→43 |
2864 measured reflections |