Oxford Diffraction Xcalibur (Sapphire2, large Be window) diffractometer	1761 independent reflections
Radiation source: Enhance (Mo) X-ray Source	1448 reflections with I > 2σ(I)
graphite	Rint = 0.022
Detector resolution: 8.1929 pixels mm-1	θmax = 26.8°, θmin = 2.3°
ω–scan	h = −8→6
Absorption correction: multi-scan (CrysAlis PRO; Oxford Diffraction, 2009)	k = −3→4
Tmin = 0.678, Tmax = 0.944	l = −31→43
2864 measured reflections