| Nonius KappaCCD diffractometer | 3136 reflections with I > 2σ(I) |
| Radiation source: rotating anode | Rint = 0.027 |
| MONTEL, graded multilayered X-ray optics | θmax = 27.5°, θmin = 3.5° |
| Detector resolution: 9 pixels mm-1 | h = −21→21 |
| CCD; rotation images; thick slices, phi/ω–scan | k = −7→6 |
| 11675 measured reflections | l = −21→20 |
| 3499 independent reflections |
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