Bruker APEXII CCD area-detector diffractometer | 6533 independent reflections |
Radiation source: fine-focus sealed tube | 3124 reflections with I > 2σ(I) |
graphite | Rint = 0.029 |
φ and ω scans | θmax = 25.0°, θmin = 1.5° |
Absorption correction: multi-scan (SADABS; Sheldrick, 1996) | h = −12→11 |
Tmin = 0.856, Tmax = 0.982 | k = −16→16 |
9908 measured reflections | l = −16→16 |