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. Author manuscript; available in PMC: 2011 Jan 4.
Published in final edited form as: Amino Acids. 2010 Jul 4;40(1):167–181. doi: 10.1007/s00726-010-0631-2

Table 1.

1H and 13C NMR chemical shifts (δ/ppm) of GLUCOLD analogue (1) in D2O

Positiona 1H (δ/ppm) 13C (δ/ppm)
2 8.66 135.8
4 – 135.0
5 7.42 121.1
1′ 5.01 62.5
2′ 3.60 71.9
3′ 3.65 70.7
4a′ 3.70 62.9
4b′ 3.52 62.9
1″ 4.04 47.4
2″ 1.74 28.8
3″ 1.14 24.8
4″ 1.47 23.5
5″ 2.24 33.5
6″ – 178.8
1‴ 4.10 49.6
2‴ 1.74 29.0
3‴ 1.20 25.0
4‴ 1.47 23.7
5‴ 2.24 33.5
6‴ – 178.8
a

Numeration see in Fig. 3

b

Chemical shifts are relative to SiMe4