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. 2001 Mar 1;29(5):1132–1143. doi: 10.1093/nar/29.5.1132

Table 2. Methyl signal line-width,ν1/2, (Hz) in different solutions of decamera.

Sample
Monovalent cation (mM)
[K+] (mM)
pH ν1/2  
 
T5
T4
T7
1 152 114 7.0  6.5  5.6  5.9
2 152b 114 7.0  7.8  4.3  6.3
  190c 114 7.0  6.7  3.8  5.3
3 152 114 7.0  4.9  4.3  4.5
4 118   0 6.0 15.0  9.0 11.1
5 228 114 6.0  7.0  4.2  5.2
6 152   0 6.0 21.1 17.0 19.7
7 190d  38 6.0 13.0 10.5 12.0

aThe line-width of TSP signal is in the range of 0.8–1.2 Hz for all studied samples. Phosphate ion concentration is 38 mM in all samples except 5, which is 76 mM in phosphate ion. Samples 1–3 are in D2O and 4–7 in H2O/D2O, 9:1 v/v.

bOriginal sample 2.

cSample 2 with 38 mM of NaCl added.

dSample 6 with 38 mM of KCl added.