Table V.

CI% for the Long-Term Stability Study at Room and Low Temperature Using the Micro-emultocrit Technique—First Run of Experiments

Formulations	MET	Storage time (day)
		D3		D5		D10		D15		D30		D60		D90		D120		D180
		R	L	R	L	R	L	R	L	R	L	R	L	R	L	R	L	R	L
F1	1.00	1.47	0.00	2.98	0.00	3.03	2.98	4.48	2.94	4.61	3.00	5.17	3.00	3.33	3.08	5.36	3.08	PS	5.80
F2	1.00	2.85	0.00	2.90	0.00	2.90	2.86	4.41	2.85	4.48	5.71	3.39	7.69	5.00	5.97	5.46	2.99	PS	3.03
F3	1.00	1.43	0.00	1.41	0.00	2.90	5.80	2.90	4.28	2.94	7.14	4.92	7.81	3.22	4.48	5.00	3.03	PS	3.03
F4	1.00	1.49	0.00	1.47	0.00	2.98	4.22	2.98	2.82	3.03	5.97	5.17	6.06	3.45	5.80	9.26	2.94	PS	4.41
F5	1.00	2.85	0.00	2.86	0.00	4.35	5.88	2.90	2.94	2.94	4.41	6.56	6.35	3.17	6.06	5.08	4.61	PS	3.08
F6	1.00	2.85	0.00	2.82	0.00	2.86	5.80	2.86	2.90	4.61	5.71	4.84	6.25	6.35	4.48	5.00	3.03	PS	3.03
F7	1.67	2.82	0.00	2.86	0.00	4.28	4.41	4.35	2.94	6.25	4.41	5.00	7.94	5.00	4.54	5.45	3.08	PS	4.35
F8	2.67	2.98	0.00	4.35	0.00	4.41	4.35	4.48	4.35	5.00	5.71	5.08	7.81	5.00	5.97	5.26	1.54	PS	4.69
F9	3.00	4.28	0.00	2.90	0.00	4.35	4.35	5.88	4.35	5.97	4.28	5.00	6.15	5.00	5.97	3.45	3.03	PS	PS
F10	3.33	5.71	0.00	5.71	0.00	5.80	4.28	7.35	4.28	7.57	5.71	6.56	7.69	8.33	PS	PS	PS	PS	PS
F11	PS	8.82	2.86	7.35	PS	10.45	PS	9.10	PS	10.00	PS	PS	PS	PS	PS	PS	PS	PS	PS
F12	PS	8.70	2.86	8.70	PS	10.29	PS	8.95	PS	11.30	PS	PS	PS	PS	PS	PS	PS	PS	PS
F13	PS	8.57	4.48	10.00	PS	10.14	PS	10.29	PS	12.30	PS	PS	PS	PS	PS	PS	PS	PS	PS
F14	PS	8.70	4.28	8.70	PS	9.10	PS	9.10	PS	11.50	PS	PS	PS	PS	PS	PS	PS	PS	PS

The relative standard deviations were lower than 5%

MET micro-emultocrit technique, PS phase separation, R room, L low, F formulation, D day