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Freeze-drying Recipe Used for 50 mg/mL Sucrose Solution
| 1 | 2 | 3 | |
|---|---|---|---|
| Freezing step | |||
| Shelf setpoint [°C] | +5 | −5 | −40 |
| Ramp rate [°C/min] | 1 | 1 | 1 |
| Time [min] | 30 | 30 | 120 |
| Primary/Secondary drying | |||
| Shelf setpoint [°C] | −25 | +40 | |
| Ramp rate [°C/min] | 0.5 | 0.3 | |
| Time [min] | 1780 | 460 | |
| Vacuum setpoint [mTorr] | 100 | 100 | |
