Table IV.
Validation of HPLC Technique for the Analysis of Carbamaz epine in Dogs Plasma
| Parameters | Values |
|---|---|
| Limit of detection (LOD; μg/ml) | 0.025 |
| Limit of quantitation (LOQ; μg/ml) | 0.25 |
| Linearity | |
| Range (μg/ml) | 0.25–4.0 |
| Regression equation | y = 4.8795 × −0.041 |
| Correlation coefficient (r) | 0.9978–0.9992 |
| Recovery range (%) | 70.45–80.43 |
| Precision | |
| Intra-day R.S.D. (%) | |
| With sample injected 3 times | 2.58 |
| With samples prepared 3 times | 3.71 |
| Inter-day R.S.D. (%) | |
| With sample injected 3 times | 5.74 |
| With samples prepared 3 times | 7.43 |