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. 2009 Jul 29;65(Pt 8):o2035. doi: 10.1107/S160053680902947X
O2A—C3A 1.353 (2) O2B—C3B 1.361 (2)
O2A—C2A 1.391 (2) O2B—C4B 1.393 (2)
O3A—C6A 1.207 (2) O3B—C8B 1.211 (2)
O4A—C8A 1.210 (2) O4B—C6B 1.212 (2)
O5A—C6A 1.364 (2) O5B—C8B 1.366 (2)
O5A—C9A 1.443 (2) O5B—C9B 1.442 (2)
O6A—C8A 1.357 (2) O6B—C6B 1.355 (2)
O6A—C9A 1.443 (2) O6B—C9B 1.446 (2)
C1A—C2A 1.382 (3) C1B—C3B 1.364 (3)
C1A—C4A 1.404 (3) C1B—C2B 1.403 (3)
C1A—H1AA 0.9300 C1B—H1BA 0.9300
C2A—C5A 1.412 (3) C2B—C4B 1.378 (3)
C3A—C4A 1.371 (3) C2B—H2BA 0.9300
C3A—C15A 1.478 (3) C3B—C15B 1.478 (3)
C4A—H4AA 0.9300 C4B—C5B 1.412 (3)
C5A—C7A 1.361 (3) C5B—C7B 1.368 (3)
C5A—H5AA 0.9300 C5B—H5BA 0.9300
C6A—C7A 1.467 (3) C6B—C7B 1.478 (3)
C7A—C8A 1.481 (3) C7B—C8B 1.463 (3)
C9A—C13A 1.508 (3) C9B—C12B 1.508 (3)
C9A—C14A 1.514 (3) C9B—C11B 1.516 (3)
C10A—C11A 1.512 (4) C10B—C14B 1.512 (4)
C10A—C14A 1.540 (3) C10B—C11B 1.534 (3)
C10A—H10A 0.9700 C10B—H10C 0.9700
C10A—H10B 0.9700 C10B—H10D 0.9700
C11A—C12A 1.534 (3) C11B—H11C 0.9700
C11A—H11A 0.9700 C11B—H11D 0.9700
C11A—H11B 0.9700 C12B—C13B 1.533 (3)
C12A—C13A 1.536 (3) C12B—H12A 0.9700
C12A—H12C 0.9700 C12B—H12B 0.9700
C12A—H12D 0.9700 C13B—C14B 1.530 (3)
C13A—H13A 0.9700 C13B—H13C 0.9700
C13A—H13B 0.9700 C13B—H13D 0.9700
C14A—H14C 0.9700 C14B—H14A 0.9700
C14A—H14D 0.9700 C14B—H14B 0.9700
C15A—H15A 0.9600 C15B—H15D 0.9600
C15A—H15B 0.9600 C15B—H15E 0.9600
C15A—H15C 0.9600 C15B—H15F 0.9600
C3A—O2A—C2A 107.65 (15) C3B—O2B—C4B 107.26 (16)
C6A—O5A—C9A 118.84 (15) C8B—O5B—C9B 119.22 (16)
C8A—O6A—C9A 118.53 (15) C6B—O6B—C9B 118.84 (15)
C2A—C1A—C4A 107.20 (18) C3B—C1B—C2B 107.22 (18)
C2A—C1A—H1AA 126.4 C3B—C1B—H1BA 126.4
C4A—C1A—H1AA 126.4 C2B—C1B—H1BA 126.4
C1A—C2A—O2A 108.14 (16) C4B—C2B—C1B 107.33 (19)
C1A—C2A—C5A 138.96 (19) C4B—C2B—H2BA 126.3
O2A—C2A—C5A 112.90 (16) C1B—C2B—H2BA 126.3
O2A—C3A—C4A 109.96 (18) O2B—C3B—C1B 109.97 (19)
O2A—C3A—C15A 117.54 (17) O2B—C3B—C15B 116.81 (18)
C4A—C3A—C15A 132.49 (18) C1B—C3B—C15B 133.19 (19)
C3A—C4A—C1A 107.04 (18) C2B—C4B—O2B 108.21 (17)
C3A—C4A—H4AA 126.5 C2B—C4B—C5B 139.2 (2)
C1A—C4A—H4AA 126.5 O2B—C4B—C5B 112.55 (17)
C7A—C5A—C2A 134.69 (18) C7B—C5B—C4B 134.40 (18)
C7A—C5A—H5AA 112.7 C7B—C5B—H5BA 112.8
C2A—C5A—H5AA 112.7 C4B—C5B—H5BA 112.8
O3A—C6A—O5A 117.86 (18) O4B—C6B—O6B 117.93 (17)
O3A—C6A—C7A 125.73 (18) O4B—C6B—C7B 125.12 (19)
O5A—C6A—C7A 116.36 (16) O6B—C6B—C7B 116.91 (17)
C5A—C7A—C6A 124.74 (17) C5B—C7B—C8B 124.97 (17)
C5A—C7A—C8A 116.08 (18) C5B—C7B—C6B 115.77 (18)
C6A—C7A—C8A 119.01 (18) C8B—C7B—C6B 119.03 (18)
O4A—C8A—O6A 118.46 (17) O3B—C8B—O5B 117.70 (18)
O4A—C8A—C7A 124.77 (19) O3B—C8B—C7B 125.61 (19)
O6A—C8A—C7A 116.72 (17) O5B—C8B—C7B 116.63 (16)
O5A—C9A—O6A 109.72 (16) O5B—C9B—O6B 110.01 (16)
O5A—C9A—C13A 111.06 (16) O5B—C9B—C12B 111.21 (17)
O6A—C9A—C13A 110.32 (17) O6B—C9B—C12B 110.41 (17)
O5A—C9A—C14A 106.51 (17) O5B—C9B—C11B 106.25 (17)
O6A—C9A—C14A 106.11 (16) O6B—C9B—C11B 105.43 (17)
C13A—C9A—C14A 112.94 (18) C12B—C9B—C11B 113.30 (18)
C11A—C10A—C14A 111.55 (18) C14B—C10B—C11B 111.61 (19)
C11A—C10A—H10A 109.3 C14B—C10B—H10C 109.3
C14A—C10A—H10A 109.3 C11B—C10B—H10C 109.3
C11A—C10A—H10B 109.3 C14B—C10B—H10D 109.3
C14A—C10A—H10B 109.3 C11B—C10B—H10D 109.3
H10A—C10A—H10B 108.0 H10C—C10B—H10D 108.0
C10A—C11A—C12A 111.68 (18) C9B—C11B—C10B 110.70 (19)
C10A—C11A—H11A 109.3 C9B—C11B—H11C 109.5
C12A—C11A—H11A 109.3 C10B—C11B—H11C 109.5
C10A—C11A—H11B 109.3 C9B—C11B—H11D 109.5
C12A—C11A—H11B 109.3 C10B—C11B—H11D 109.5
H11A—C11A—H11B 107.9 H11C—C11B—H11D 108.1
C11A—C12A—C13A 111.25 (18) C9B—C12B—C13B 111.01 (18)
C11A—C12A—H12C 109.4 C9B—C12B—H12A 109.4
C13A—C12A—H12C 109.4 C13B—C12B—H12A 109.4
C11A—C12A—H12D 109.4 C9B—C12B—H12B 109.4
C13A—C12A—H12D 109.4 C13B—C12B—H12B 109.4
H12C—C12A—H12D 108.0 H12A—C12B—H12B 108.0
C9A—C13A—C12A 110.95 (17) C14B—C13B—C12B 111.74 (19)
C9A—C13A—H13A 109.4 C14B—C13B—H13C 109.3
C12A—C13A—H13A 109.4 C12B—C13B—H13C 109.3
C9A—C13A—H13B 109.4 C14B—C13B—H13D 109.3
C12A—C13A—H13B 109.4 C12B—C13B—H13D 109.3
H13A—C13A—H13B 108.0 H13C—C13B—H13D 107.9
C9A—C14A—C10A 110.81 (18) C10B—C14B—C13B 111.28 (18)
C9A—C14A—H14C 109.5 C10B—C14B—H14A 109.4
C10A—C14A—H14C 109.5 C13B—C14B—H14A 109.4
C9A—C14A—H14D 109.5 C10B—C14B—H14B 109.4
C10A—C14A—H14D 109.5 C13B—C14B—H14B 109.4
H14C—C14A—H14D 108.1 H14A—C14B—H14B 108.0
C3A—C15A—H15A 109.5 C3B—C15B—H15D 109.5
C3A—C15A—H15B 109.5 C3B—C15B—H15E 109.5
H15A—C15A—H15B 109.5 H15D—C15B—H15E 109.5
C3A—C15A—H15C 109.5 C3B—C15B—H15F 109.5
H15A—C15A—H15C 109.5 H15D—C15B—H15F 109.5
H15B—C15A—H15C 109.5 H15E—C15B—H15F 109.5