| Bruker SMART CCD area-detector diffractometer | 6028 independent reflections |
| Radiation source: fine-focus sealed tube | 3716 reflections with I > 2σ(I) |
| graphite | Rint = 0.049 |
| φ and ω scans | θmax = 27.5°, θmin = 3.1° |
| Absorption correction: multi-scan (SADABS; Sheldrick, 1996) | h = −25→24 |
| Tmin = 0.978, Tmax = 0.985 | k = −8→8 |
| 21978 measured reflections | l = −26→26 |