Rigaku R-AXIS RAPID IP diffractometer | 2997 independent reflections |
Radiation source: fine-focus sealed tube | 2638 reflections with I > 2σ(I) |
graphite | Rint = 0.024 |
Detector resolution: 10.0 pixels mm-1 | θmax = 27.4°, θmin = 3.0° |
ω scans | h = −15→15 |
Absorption correction: multi-scan (ABSCOR; Higashi, 1995) | k = −10→10 |
Tmin = 0.635, Tmax = 0.720 | l = −17→17 |
12480 measured reflections |