Cu1—O1 | 2.105 (5) | C17—H17 | 0.9300 |
Cu1—P1 | 2.2318 (18) | C18—H18 | 0.9300 |
Cu1—P2 | 2.2478 (18) | C19—C24 | 1.375 (9) |
O1—H1C | 0.8500 | C19—C20 | 1.389 (9) |
O1—H1D | 0.8500 | C20—C21 | 1.366 (10) |
P1—C13 | 1.800 (7) | C20—H20 | 0.9300 |
P1—C7 | 1.816 (6) | C21—C22 | 1.349 (10) |
P1—C1 | 1.823 (6) | C21—H21 | 0.9300 |
P2—C19 | 1.803 (7) | C22—C23 | 1.368 (10) |
P2—C31 | 1.814 (6) | C22—H22 | 0.9300 |
P2—C25 | 1.820 (6) | C23—C24 | 1.377 (10) |
C1—C6 | 1.383 (8) | C23—H23 | 0.9300 |
C1—C2 | 1.400 (9) | C24—H24 | 0.9300 |
C2—C3 | 1.366 (9) | C25—C30 | 1.380 (9) |
C2—H2 | 0.9300 | C25—C26 | 1.382 (9) |
C3—C4 | 1.357 (10) | C26—C27 | 1.410 (10) |
C3—H3 | 0.9300 | C26—H26 | 0.9300 |
C4—C5 | 1.378 (10) | C27—C28 | 1.373 (11) |
C4—H4 | 0.9300 | C27—H27 | 0.9300 |
C5—C6 | 1.385 (9) | C28—C29 | 1.355 (11) |
C5—H5 | 0.9300 | C28—H28 | 0.9300 |
C6—H6 | 0.9300 | C29—C30 | 1.375 (9) |
C7—C12 | 1.373 (9) | C29—H29 | 0.9300 |
C7—C8 | 1.394 (9) | C30—H30 | 0.9300 |
C8—C9 | 1.374 (9) | C31—C32 | 1.367 (9) |
C8—H8 | 0.9300 | C31—C36 | 1.390 (9) |
C9—C10 | 1.350 (10) | C32—C33 | 1.391 (9) |
C9—H9 | 0.9300 | C32—H32 | 0.9300 |
C10—C11 | 1.362 (10) | C33—C34 | 1.369 (10) |
C10—H10 | 0.9300 | C33—H33 | 0.9300 |
C11—C12 | 1.391 (10) | C34—C35 | 1.351 (10) |
C11—H11 | 0.9300 | C34—H34 | 0.9300 |
C12—H12 | 0.9300 | C35—C36 | 1.381 (9) |
C13—C14 | 1.374 (9) | C35—H35 | 0.9300 |
C13—C18 | 1.377 (9) | C36—H36 | 0.9300 |
C14—C15 | 1.393 (11) | B1—F4 | 1.285 (19) |
C14—H14 | 0.9300 | B1—F2' | 1.30 (3) |
C15—C16 | 1.354 (12) | B1—F4' | 1.31 (5) |
C15—H15 | 0.9300 | B1—F1 | 1.363 (12) |
C16—C17 | 1.352 (11) | B1—F2 | 1.38 (3) |
C16—H16 | 0.9300 | B1—F3 | 1.42 (2) |
C17—C18 | 1.370 (10) | B1—F3' | 1.48 (4) |
O1—Cu1—P1 | 115.18 (16) | C17—C18—C13 | 122.6 (7) |
O1—Cu1—P2 | 104.80 (16) | C17—C18—H18 | 118.7 |
P1—Cu1—P2 | 133.89 (7) | C13—C18—H18 | 118.7 |
Cu1—O1—H1C | 106.5 | C24—C19—C20 | 117.0 (7) |
Cu1—O1—H1D | 139.8 | C24—C19—P2 | 124.6 (5) |
H1C—O1—H1D | 108.6 | C20—C19—P2 | 118.1 (5) |
C13—P1—C7 | 106.4 (3) | C21—C20—C19 | 121.1 (7) |
C13—P1—C1 | 104.2 (3) | C21—C20—H20 | 119.4 |
C7—P1—C1 | 102.2 (3) | C19—C20—H20 | 119.4 |
C13—P1—Cu1 | 106.8 (2) | C22—C21—C20 | 120.8 (8) |
C7—P1—Cu1 | 119.8 (2) | C22—C21—H21 | 119.6 |
C1—P1—Cu1 | 116.1 (2) | C20—C21—H21 | 119.6 |
C19—P2—C31 | 104.8 (3) | C21—C22—C23 | 119.7 (8) |
C19—P2—C25 | 101.7 (3) | C21—C22—H22 | 120.2 |
C31—P2—C25 | 103.9 (3) | C23—C22—H22 | 120.2 |
C19—P2—Cu1 | 110.4 (2) | C22—C23—C24 | 119.8 (8) |
C31—P2—Cu1 | 119.0 (2) | C22—C23—H23 | 120.1 |
C25—P2—Cu1 | 115.2 (2) | C24—C23—H23 | 120.1 |
C6—C1—C2 | 118.0 (6) | C19—C24—C23 | 121.5 (7) |
C6—C1—P1 | 123.7 (5) | C19—C24—H24 | 119.2 |
C2—C1—P1 | 118.3 (5) | C23—C24—H24 | 119.2 |
C3—C2—C1 | 121.3 (7) | C30—C25—C26 | 118.0 (6) |
C3—C2—H2 | 119.4 | C30—C25—P2 | 123.2 (5) |
C1—C2—H2 | 119.4 | C26—C25—P2 | 118.8 (6) |
C4—C3—C2 | 120.3 (7) | C25—C26—C27 | 120.2 (8) |
C4—C3—H3 | 119.8 | C25—C26—H26 | 119.9 |
C2—C3—H3 | 119.8 | C27—C26—H26 | 119.9 |
C3—C4—C5 | 119.8 (7) | C28—C27—C26 | 119.4 (8) |
C3—C4—H4 | 120.1 | C28—C27—H27 | 120.3 |
C5—C4—H4 | 120.1 | C26—C27—H27 | 120.3 |
C4—C5—C6 | 120.7 (7) | C29—C28—C27 | 120.6 (8) |
C4—C5—H5 | 119.7 | C29—C28—H28 | 119.7 |
C6—C5—H5 | 119.7 | C27—C28—H28 | 119.7 |
C1—C6—C5 | 119.9 (6) | C28—C29—C30 | 119.8 (8) |
C1—C6—H6 | 120.0 | C28—C29—H29 | 120.1 |
C5—C6—H6 | 120.0 | C30—C29—H29 | 120.1 |
C12—C7—C8 | 117.6 (6) | C29—C30—C25 | 121.9 (7) |
C12—C7—P1 | 119.6 (5) | C29—C30—H30 | 119.0 |
C8—C7—P1 | 122.8 (5) | C25—C30—H30 | 119.0 |
C9—C8—C7 | 121.3 (7) | C32—C31—C36 | 117.2 (6) |
C9—C8—H8 | 119.4 | C32—C31—P2 | 119.7 (5) |
C7—C8—H8 | 119.4 | C36—C31—P2 | 123.0 (5) |
C10—C9—C8 | 119.8 (7) | C31—C32—C33 | 122.0 (7) |
C10—C9—H9 | 120.1 | C31—C32—H32 | 119.0 |
C8—C9—H9 | 120.1 | C33—C32—H32 | 119.0 |
C9—C10—C11 | 120.9 (7) | C34—C33—C32 | 118.9 (7) |
C9—C10—H10 | 119.6 | C34—C33—H33 | 120.5 |
C11—C10—H10 | 119.6 | C32—C33—H33 | 120.5 |
C10—C11—C12 | 119.6 (7) | C35—C34—C33 | 120.6 (7) |
C10—C11—H11 | 120.2 | C35—C34—H34 | 119.7 |
C12—C11—H11 | 120.2 | C33—C34—H34 | 119.7 |
C7—C12—C11 | 120.8 (7) | C34—C35—C36 | 120.1 (7) |
C7—C12—H12 | 119.6 | C34—C35—H35 | 120.0 |
C11—C12—H12 | 119.6 | C36—C35—H35 | 120.0 |
C14—C13—C18 | 117.2 (7) | C35—C36—C31 | 121.2 (7) |
C14—C13—P1 | 123.8 (6) | C35—C36—H36 | 119.4 |
C18—C13—P1 | 118.9 (5) | C31—C36—H36 | 119.4 |
C13—C14—C15 | 120.0 (8) | F4—B1—F1 | 112.3 (13) |
C13—C14—H14 | 120.0 | F4—B1—F2 | 114.1 (18) |
C15—C14—H14 | 120.0 | F1—B1—F2 | 107.7 (14) |
C16—C15—C14 | 120.7 (8) | F4—B1—F3 | 110.3 (14) |
C16—C15—H15 | 119.6 | F1—B1—F3 | 103.1 (12) |
C14—C15—H15 | 119.6 | F2—B1—F3 | 108.8 (13) |
C17—C16—C15 | 120.2 (9) | F2'—B1—F4' | 104 (3) |
C17—C16—H16 | 119.9 | F2'—B1—F3' | 103 (2) |
C15—C16—H16 | 119.9 | F4'—B1—F3' | 106 (3) |
C16—C17—C18 | 119.2 (8) | F1—B1—F3' | 105.6 (16) |
C16—C17—H17 | 120.4 | F2'—B1—F1 | 120 (2) |
C18—C17—H17 | 120.4 | F4'—B1—F1 | 117 (3) |
O1—Cu1—P1—C13 | 75.2 (3) | C13—C14—C15—C16 | 1.1 (15) |
P2—Cu1—P1—C13 | −72.4 (2) | C14—C15—C16—C17 | −1.5 (17) |
O1—Cu1—P1—C7 | −45.7 (3) | C15—C16—C17—C18 | 0.6 (17) |
P2—Cu1—P1—C7 | 166.8 (2) | C16—C17—C18—C13 | 0.8 (15) |
O1—Cu1—P1—C1 | −169.2 (3) | C14—C13—C18—C17 | −1.3 (12) |
P2—Cu1—P1—C1 | 43.3 (3) | P1—C13—C18—C17 | −177.8 (7) |
O1—Cu1—P2—C19 | −83.8 (3) | C31—P2—C19—C24 | −10.6 (7) |
P1—Cu1—P2—C19 | 66.0 (2) | C25—P2—C19—C24 | 97.4 (6) |
O1—Cu1—P2—C31 | 155.1 (3) | Cu1—P2—C19—C24 | −139.8 (5) |
P1—Cu1—P2—C31 | −55.1 (3) | C31—P2—C19—C20 | 175.1 (5) |
O1—Cu1—P2—C25 | 30.6 (3) | C25—P2—C19—C20 | −76.9 (6) |
P1—Cu1—P2—C25 | −179.5 (2) | Cu1—P2—C19—C20 | 45.8 (6) |
C13—P1—C1—C6 | −26.4 (6) | C24—C19—C20—C21 | −3.0 (11) |
C7—P1—C1—C6 | 84.2 (6) | P2—C19—C20—C21 | 171.7 (6) |
Cu1—P1—C1—C6 | −143.5 (5) | C19—C20—C21—C22 | 1.4 (13) |
C13—P1—C1—C2 | 156.7 (5) | C20—C21—C22—C23 | 1.4 (13) |
C7—P1—C1—C2 | −92.7 (5) | C21—C22—C23—C24 | −2.4 (13) |
Cu1—P1—C1—C2 | 39.6 (6) | C20—C19—C24—C23 | 2.0 (11) |
C6—C1—C2—C3 | 1.0 (10) | P2—C19—C24—C23 | −172.4 (6) |
P1—C1—C2—C3 | 178.1 (6) | C22—C23—C24—C19 | 0.7 (12) |
C1—C2—C3—C4 | −0.8 (11) | C19—P2—C25—C30 | −28.7 (6) |
C2—C3—C4—C5 | −0.3 (12) | C31—P2—C25—C30 | 80.0 (6) |
C3—C4—C5—C6 | 1.1 (11) | Cu1—P2—C25—C30 | −148.0 (5) |
C2—C1—C6—C5 | −0.2 (10) | C19—P2—C25—C26 | 153.1 (5) |
P1—C1—C6—C5 | −177.1 (5) | C31—P2—C25—C26 | −98.3 (6) |
C4—C5—C6—C1 | −0.8 (11) | Cu1—P2—C25—C26 | 33.7 (6) |
C13—P1—C7—C12 | −111.1 (6) | C30—C25—C26—C27 | −1.5 (10) |
C1—P1—C7—C12 | 139.9 (6) | P2—C25—C26—C27 | 176.8 (6) |
Cu1—P1—C7—C12 | 10.0 (7) | C25—C26—C27—C28 | −0.4 (12) |
C13—P1—C7—C8 | 72.0 (6) | C26—C27—C28—C29 | 2.3 (13) |
C1—P1—C7—C8 | −37.0 (6) | C27—C28—C29—C30 | −2.2 (12) |
Cu1—P1—C7—C8 | −166.9 (5) | C28—C29—C30—C25 | 0.2 (11) |
C12—C7—C8—C9 | −0.7 (10) | C26—C25—C30—C29 | 1.6 (10) |
P1—C7—C8—C9 | 176.2 (6) | P2—C25—C30—C29 | −176.6 (5) |
C7—C8—C9—C10 | 1.3 (11) | C19—P2—C31—C32 | −81.9 (6) |
C8—C9—C10—C11 | −1.5 (13) | C25—P2—C31—C32 | 171.8 (6) |
C9—C10—C11—C12 | 1.1 (13) | Cu1—P2—C31—C32 | 42.0 (7) |
C8—C7—C12—C11 | 0.3 (11) | C19—P2—C31—C36 | 100.8 (6) |
P1—C7—C12—C11 | −176.7 (6) | C25—P2—C31—C36 | −5.5 (7) |
C10—C11—C12—C7 | −0.5 (13) | Cu1—P2—C31—C36 | −135.3 (6) |
C7—P1—C13—C14 | 12.0 (7) | C36—C31—C32—C33 | −1.2 (11) |
C1—P1—C13—C14 | 119.6 (6) | P2—C31—C32—C33 | −178.7 (6) |
Cu1—P1—C13—C14 | −117.1 (6) | C31—C32—C33—C34 | 1.3 (12) |
C7—P1—C13—C18 | −171.7 (6) | C32—C33—C34—C35 | −0.3 (13) |
C1—P1—C13—C18 | −64.2 (6) | C33—C34—C35—C36 | −0.7 (13) |
Cu1—P1—C13—C18 | 59.2 (6) | C34—C35—C36—C31 | 0.8 (13) |
C18—C13—C14—C15 | 0.3 (12) | C32—C31—C36—C35 | 0.1 (11) |
P1—C13—C14—C15 | 176.6 (7) | P2—C31—C36—C35 | 177.5 (6) |