| Bruker SMART APEXII area-detector diffractometer | 5914 independent reflections |
| Radiation source: fine-focus sealed tube | 3008 reflections with I > 2σ(I) |
| graphite | Rint = 0.078 |
| φ and ω scans | θmax = 25.0°, θmin = 1.7° |
| Absorption correction: multi-scan (SADABS; Sheldrick, 1996) | h = −16→15 |
| Tmin = 0.702, Tmax = 0.883 | k = −14→14 |
| 17192 measured reflections | l = −23→22 |
Official websites use .gov
A
.gov website belongs to an official
government organization in the United States.
Secure .gov websites use HTTPS
A lock (
) or https:// means you've safely
connected to the .gov website. Share sensitive
information only on official, secure websites.