Bruker SMART APEX diffractometer | 12754 independent reflections |
Radiation source: fine-focus sealed tube | 9841 reflections with I > 2σ(I) |
graphite | Rint = 0.045 |
ω scans | θmax = 27.5°, θmin = 1.2° |
Absorption correction: multi-scan (SADABS; Sheldrick, 1996) | h = −15→15 |
Tmin = 0.642, Tmax = 0.746 | k = −17→17 |
23151 measured reflections | l = −21→21 |