| Stoe IPDS-II two-circle diffractometer | 3580 independent reflections |
| Radiation source: fine-focus sealed tube | 3067 reflections with I > 2σ(I) |
| graphite | Rint = 0.053 |
| ω scans | θmax = 27.1°, θmin = 2.9° |
| Absorption correction: multi-scan (MULABS; Spek, 2009; Blessing, 1995) | h = −6→7 |
| Tmin = 0.546, Tmax = 0.581 | k = −22→22 |
| 25973 measured reflections | l = −19→19 |
Official websites use .gov
A
.gov website belongs to an official
government organization in the United States.
Secure .gov websites use HTTPS
A lock (
) or https:// means you've safely
connected to the .gov website. Share sensitive
information only on official, secure websites.