Ni1—O1 | 1.838 (2) | C3—C4 | 1.371 (5) |
Ni1—N2 | 1.839 (3) | C4—C5 | 1.387 (6) |
Ni1—N1 | 1.840 (3) | C4—H4 | 0.9300 |
Ni1—O2 | 1.8457 (19) | C5—C6 | 1.361 (7) |
Na1—O5 | 2.288 (2) | C5—H5 | 0.9300 |
Na1—O1 | 2.362 (2) | C6—H6 | 0.9300 |
Na1—N5 | 2.368 (4) | C7—H7 | 0.9300 |
Na1—O2 | 2.395 (2) | C8—H8A | 0.9600 |
Na1—O3 | 2.492 (3) | C8—H8B | 0.9600 |
Na1—O4 | 2.555 (2) | C8—H8C | 0.9600 |
O1—C10 | 1.314 (4) | C9—C10 | 1.412 (4) |
O2—C2 | 1.310 (3) | C9—C16 | 1.413 (5) |
O3—C11 | 1.365 (4) | C9—C14 | 1.419 (5) |
O3—C15 | 1.420 (4) | C10—C11 | 1.410 (5) |
O4—C3 | 1.365 (4) | C11—C12 | 1.375 (5) |
O4—C8 | 1.429 (4) | C12—C13 | 1.389 (6) |
O5—H5A | 0.8200 | C12—H12 | 0.9300 |
O5—H5B | 0.8246 | C13—C14 | 1.349 (6) |
N1—C16 | 1.276 (4) | C13—H13 | 0.9300 |
N1—C17 | 1.476 (4) | C14—H14 | 0.9300 |
N2—C7 | 1.282 (4) | C15—H15A | 0.9600 |
N2—C18 | 1.468 (5) | C15—H15B | 0.9600 |
N3—C19 | 1.292 (5) | C15—H15C | 0.9600 |
N3—C20 | 1.297 (5) | C17—C18 | 1.436 (6) |
N4—C19 | 1.127 (4) | C17—H16A | 0.9700 |
N5—C20 | 1.127 (4) | C17—H16B | 0.9700 |
C1—C6 | 1.405 (5) | C18—H17A | 0.9700 |
C1—C2 | 1.411 (5) | C18—H17B | 0.9700 |
C1—C7 | 1.425 (5) | C16—H20 | 0.9300 |
C2—C3 | 1.419 (5) | ||
O1—Ni1—N2 | 178.09 (11) | C6—C5—C4 | 120.6 (4) |
O1—Ni1—N1 | 94.79 (11) | C6—C5—H5 | 119.7 |
N2—Ni1—N1 | 86.76 (14) | C4—C5—H5 | 119.7 |
O1—Ni1—O2 | 83.62 (9) | C5—C6—C1 | 120.5 (4) |
N2—Ni1—O2 | 94.82 (11) | C5—C6—H6 | 119.7 |
N1—Ni1—O2 | 178.41 (11) | C1—C6—H6 | 119.7 |
O5—Na1—O1 | 120.42 (9) | N2—C7—C1 | 125.7 (3) |
O5—Na1—N5 | 101.85 (12) | N2—C7—H7 | 117.1 |
O1—Na1—N5 | 127.99 (12) | C1—C7—H7 | 117.1 |
O5—Na1—O2 | 116.86 (9) | O4—C8—H8A | 109.5 |
O1—Na1—O2 | 62.15 (7) | O4—C8—H8B | 109.5 |
N5—Na1—O2 | 124.88 (11) | H8A—C8—H8B | 109.5 |
O5—Na1—O3 | 90.51 (9) | O4—C8—H8C | 109.5 |
O1—Na1—O3 | 64.15 (8) | H8A—C8—H8C | 109.5 |
N5—Na1—O3 | 88.43 (11) | H8B—C8—H8C | 109.5 |
O2—Na1—O3 | 126.30 (8) | C10—C9—C16 | 121.1 (3) |
O5—Na1—O4 | 84.15 (8) | C10—C9—C14 | 118.6 (4) |
O1—Na1—O4 | 124.77 (9) | C16—C9—C14 | 120.2 (4) |
N5—Na1—O4 | 85.68 (11) | O1—C10—C11 | 118.0 (3) |
O2—Na1—O4 | 62.63 (7) | O1—C10—C9 | 123.4 (3) |
O3—Na1—O4 | 171.07 (9) | C11—C10—C9 | 118.6 (3) |
C10—O1—Ni1 | 127.8 (2) | O3—C11—C12 | 125.5 (4) |
C10—O1—Na1 | 124.3 (2) | O3—C11—C10 | 113.8 (3) |
Ni1—O1—Na1 | 107.87 (9) | C12—C11—C10 | 120.7 (4) |
C2—O2—Ni1 | 127.3 (2) | C11—C12—C13 | 120.4 (4) |
C2—O2—Na1 | 125.61 (19) | C11—C12—H12 | 119.8 |
Ni1—O2—Na1 | 106.26 (9) | C13—C12—H12 | 119.8 |
C11—O3—C15 | 118.3 (3) | C14—C13—C12 | 120.3 (4) |
C11—O3—Na1 | 119.68 (19) | C14—C13—H13 | 119.8 |
C15—O3—Na1 | 122.0 (2) | C12—C13—H13 | 119.8 |
C3—O4—C8 | 118.2 (3) | C13—C14—C9 | 121.3 (4) |
C3—O4—Na1 | 119.73 (19) | C13—C14—H14 | 119.3 |
C8—O4—Na1 | 122.1 (2) | C9—C14—H14 | 119.3 |
Na1—O5—H5A | 130.6 | O3—C15—H15A | 109.5 |
Na1—O5—H5B | 118.8 | O3—C15—H15B | 109.5 |
H5A—O5—H5B | 110.0 | H15A—C15—H15B | 109.5 |
C16—N1—C17 | 119.2 (3) | O3—C15—H15C | 109.5 |
C16—N1—Ni1 | 126.4 (2) | H15A—C15—H15C | 109.5 |
C17—N1—Ni1 | 114.3 (3) | H15B—C15—H15C | 109.5 |
C7—N2—C18 | 118.9 (3) | C18—C17—N1 | 110.7 (3) |
C7—N2—Ni1 | 126.8 (3) | C18—C17—H16A | 109.5 |
C18—N2—Ni1 | 114.2 (3) | N1—C17—H16A | 109.5 |
C19—N3—C20 | 120.5 (3) | C18—C17—H16B | 109.5 |
C20—N5—Na1 | 171.8 (4) | N1—C17—H16B | 109.5 |
C6—C1—C2 | 119.6 (4) | H16A—C17—H16B | 108.1 |
C6—C1—C7 | 119.2 (4) | C17—C18—N2 | 111.4 (3) |
C2—C1—C7 | 121.1 (3) | C17—C18—H17A | 109.4 |
O2—C2—C1 | 123.9 (3) | N2—C18—H17A | 109.4 |
O2—C2—C3 | 117.9 (3) | C17—C18—H17B | 109.4 |
C1—C2—C3 | 118.2 (3) | N2—C18—H17B | 109.4 |
O4—C3—C4 | 126.1 (4) | H17A—C18—H17B | 108.0 |
O4—C3—C2 | 113.4 (3) | N4—C19—N3 | 173.6 (4) |
C4—C3—C2 | 120.4 (4) | N5—C20—N3 | 173.8 (4) |
C3—C4—C5 | 120.5 (4) | N1—C16—C9 | 126.5 (3) |
C3—C4—H4 | 119.7 | N1—C16—H20 | 116.7 |
C5—C4—H4 | 119.7 | C9—C16—H20 | 116.7 |