| Bruker SMART 1K CCD area-detector diffractometer | 979 independent reflections |
| Radiation source: fine-focus sealed tube | 724 reflections with I > 2σ(I) |
| graphite | Rint = 0.075 |
| ω scans | θmax = 25.0°, θmin = 2.1° |
| Absorption correction: multi-scan (SADABS; Bruker, 2000) | h = −9→11 |
| Tmin = 0.989, Tmax = 0.992 | k = −6→8 |
| 2698 measured reflections | l = −8→9 |
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