| Bruker APEXII CCD diffractometer | 3365 independent reflections |
| Radiation source: sealed tube | 3060 reflections with I > 2σ(I) |
| graphite | Rint = 0.029 |
| φ and ω scans | θmax = 26.0°, θmin = 2.3° |
| Absorption correction: multi-scan (SADABS; Bruker, 2000) | h = −12→12 |
| Tmin = 0.885, Tmax = 0.988 | k = −13→13 |
| 20360 measured reflections | l = −19→19 |