| Bruker X8 APEXII CCD area-detector diffractometer | 2358 reflections with I > 2σ(I) |
| Radiation source: fine-focus sealed tube | Rint = 0.023 |
| graphite | θmax = 27.5°, θmin = 2.8° |
| φ and ω scans | h = −9→9 |
| 15358 measured reflections | k = −9→9 |
| 3030 independent reflections | l = −17→17 |
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