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. 2010 Apr 21;66(Pt 5):m546–m547. doi: 10.1107/S1600536810013772

Table 1. Geometrical parameters (Å, °) of the environment of the Ti atom in the title compound compared with those of related structures.

  (I) (III) (IV) (V) (VI)
Ti1—N2 2.153 (2) 2.163 (2) 2.357 (1) 2.274 (4) 2.261 (2)
Ti1—Cl1 2.3475 (9) 2.3513 (8) 2.3217 (4) 2.322 (2) 2.331 (1)
Ti1—Cl2 2.3377 (10) 2.3486 (8) 2.3729 (5) 2.326 (2) 2.338 (1)
Ti1—Cl3 2.3533 (9) 2.3340 (8) 2.2895 (5) 2.300 (2) 2.307 (1)
Ti1⋯Cpcent 2.030 (1) 2.036 2.025 2.035 2.047
Ti1⋯PL1 2.029 (1) 2.034 (1) 2.025 2.034 2.046
Ti1⋯PL2 0.022 (5) 0.608   0.175 0.215
N2—Ti1⋯Cpcent 111.2 (1)a 110.20 99.66 101.44 101.64
Cl1—Ti1⋯Cpcent 109.2 (1)a 110.08 116.37 116.68 113.90
Cl2—Ti1⋯Cpcent 110.69 (9)a 109.75 107.63 109.28 109.73
Cl3—Ti1⋯Cpcent 110.58 (9)a 110.93 114.71 113.76 115.56
Cl1—Ti1—N2 80.79 (7) 79.24 (6) 82.57 (2) 78.64 80.32
Cl2—Ti1—N2 138.10 (6) 140.05 (6) 152.70 (3) 149.27 148.63
Cl3—Ti1—N2 80.82 (7) 81.19 (6) 83.45 (2) 80.23 78.94
Cl2—Ti1—Cl1 85.38 (4) 86.06 (3) 85.18 (2) 87.84 87.14
Cl2—Ti1—Cl3 85.07 (4) 86.01 (3) 85.30 (2) 86.95 87.20
Cl3—Ti1—Cl1 139.98 (4) 138.52 (3) 128.55 (2) 128.07 129.12
PL1–PL2 81.0 (1) 78.335   82.491 85.895

Notes: (a) the angle between the Ti1—N2 bond and the normal to PL1; (I) this work; (III) Krut’ko et al. (2006); (IV) Herrmann et al. (1995); (V) Enders et al. (1997); (VI) Enders et al. (1996). PL1 and Cpcent denote the C11–C15 Cp ring r.m.s. plane and centroid, respectively, while PL2 denotes an r.m.s. plane through the non-H atoms of a heterocyclic ring.