| Nonius KappaCCD diffractometer | 3041 independent reflections |
| Radiation source: fine-focus sealed tube | 1939 reflections with I > 2σ(I) |
| graphite | Rint = 0.079 |
| Detector resolution: 18 pixels mm-1 | θmax = 26.0°, θmin = 2.3° |
| ω scans at fixed χ = 55° | h = −9→9 |
| Absorption correction: multi-scan (SADABS; Bruker Nonius, 2006) | k = −7→7 |
| Tmin = 0.699, Tmax = 0.944 | l = −43→43 |
| 15429 measured reflections |
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