Table 2. Hydrogen-bond geometry (Å, °).
| D—H⋯A | D—H | H⋯A | D⋯A | D—H⋯A |
|---|---|---|---|---|
| N1—H11N⋯O17 | 0.86 (3) | 2.00 (3) | 2.836 (3) | 165 (3) |
| N1—H12N⋯O7 | 0.81 (3) | 1.98 (3) | 2.785 (2) | 175 (3) |
| N1—H13N⋯O15i | 0.85 (3) | 1.98 (3) | 2.810 (2) | 165 (3) |
| N2—H21N⋯O23A | 0.91 (3) | 1.94 (3) | 2.808 (4) | 159 (3) |
| N2—H22N⋯O4 | 0.90 (3) | 2.05 (3) | 2.944 (2) | 173 (3) |
| N2—H23N⋯O16 | 0.90 (3) | 1.90 (3) | 2.783 (3) | 164 (3) |
| O3—H3O⋯O6ii | 0.66 (3) | 1.92 (3) | 2.570 (2) | 169 (4) |
| O5—H5O⋯O2i | 0.76 (3) | 1.84 (3) | 2.592 (2) | 170 (3) |
| O8—H8O⋯O11iii | 0.70 (3) | 1.81 (3) | 2.508 (2) | 169 (3) |
| O12—H12O⋯O9iv | 0.83 (3) | 1.71 (3) | 2.517 (2) | 165 (3) |
| O13—H131⋯O6ii | 0.79 (3) | 1.92 (3) | 2.691 (2) | 166 (3) |
| O13—H132⋯O20A | 0.77 (3) | 1.92 (3) | 2.671 (3) | 165 (3) |
| O14—H141⋯O18Av | 0.82 (3) | 1.91 (3) | 2.697 (3) | 163 (3) |
| O14—H142⋯O9iv | 0.74 (3) | 1.95 (3) | 2.688 (2) | 172 (3) |
| O15—H151⋯O1 | 0.80 (3) | 2.01 (3) | 2.803 (2) | 177 (3) |
| O15—H152⋯O14 | 0.66 (3) | 2.50 (3) | 2.946 (2) | 127 (3) |
| O15—H152⋯O12iv | 0.66 (3) | 2.54 (3) | 3.049 (2) | 136 (3) |
| O16—H161⋯O15i | 0.85 (4) | 1.94 (4) | 2.788 (3) | 176 (3) |
| O16—H162⋯O17i | 0.89 (4) | 1.97 (4) | 2.844 (3) | 170 (3) |
| O17—H171⋯O21vi | 0.75 (3) | 2.14 (4) | 2.795 (3) | 147 (3) |
| O17—H172⋯O18Avii | 0.73 (4) | 2.13 (4) | 2.845 (3) | 167 (4) |
| O19—H191⋯O13 | 0.84 (4) | 2.27 (4) | 3.063 (3) | 158 (3) |
| O19—H192⋯O2v | 0.75 (4) | 2.04 (4) | 2.773 (3) | 166 (4) |
| O21—H211⋯O19 | 0.80 (4) | 2.05 (4) | 2.815 (3) | 162 (4) |
| O21—H212⋯O19viii | 1.00 (4) | 1.93 (4) | 2.914 (3) | 169 (3) |
Symmetry codes: (i)
; (ii)
; (iii)
; (iv)
; (v)
; (vi)
; (vii)
; (viii)
.