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. 2010 Apr 28;66(Pt 5):o1194–o1195. doi: 10.1107/S1600536810014480
Bruker APEX DUO CCD area-detector diffractometer 4947 independent reflections
Radiation source: fine-focus sealed tube 3922 reflections with I > 2σ(I)
graphite Rint = 0.023
φ and ω scans θmax = 32.5°, θmin = 1.3°
Absorption correction: multi-scan (SADABS; Bruker, 2009) h = −8→8
Tmin = 0.963, Tmax = 0.990 k = −12→11
12709 measured reflections l = −22→23