Bruker APEX DUO CCD area-detector diffractometer | 4947 independent reflections |
Radiation source: fine-focus sealed tube | 3922 reflections with I > 2σ(I) |
graphite | Rint = 0.023 |
φ and ω scans | θmax = 32.5°, θmin = 1.3° |
Absorption correction: multi-scan (SADABS; Bruker, 2009) | h = −8→8 |
Tmin = 0.963, Tmax = 0.990 | k = −12→11 |
12709 measured reflections | l = −22→23 |