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. 2010 May 26;66(Pt 6):o1446–o1447. doi: 10.1107/S1600536810018647
Refinement on F2 Primary atom site location: structure-invariant direct methods
Least-squares matrix: full Secondary atom site location: difference Fourier map
R[F2 > 2σ(F2)] = 0.044 Hydrogen site location: inferred from neighbouring sites
wR(F2) = 0.102 H atoms treated by a mixture of independent and constrained refinement
S = 1.04 w = 1/[σ2(Fo2) + (0.0409P)2 + 0.4898P] where P = (Fo2 + 2Fc2)/3
2855 reflections (Δ/σ)max < 0.001
239 parameters Δρmax = 0.22 e Å3
0 restraints Δρmin = −0.33 e Å3