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. 2010 May 29;66(Pt 6):o1498–o1499. doi: 10.1107/S1600536810019653
Refinement on F2 Primary atom site location: structure-invariant direct methods
Least-squares matrix: full Secondary atom site location: difference Fourier map
R[F2 > 2σ(F2)] = 0.048 Hydrogen site location: inferred from neighbouring sites
wR(F2) = 0.128 H-atom parameters constrained
S = 1.06 w = 1/[σ2(Fo2) + (0.0407P)2 + 2.6662P] where P = (Fo2 + 2Fc2)/3
7564 reflections (Δ/σ)max < 0.001
480 parameters Δρmax = 0.94 e Å3
0 restraints Δρmin = −0.31 e Å3