| Bruker SMART APEXII area-detector diffractometer | 4398 independent reflections |
| Radiation source: fine-focus sealed tube | 2725 reflections with I > 2σ(I) |
| graphite | Rint = 0.035 |
| ω and φ scans | θmax = 28.5°, θmin = 1.8° |
| Absorption correction: multi-scan (SADABS; Bruker, 2008) | h = −27→28 |
| Tmin = 0.499, Tmax = 0.596 | k = −19→19 |
| 17094 measured reflections | l = −18→18 |