Table 1. Hydrogen-bond geometry (Å, °).
| D—H⋯A | D—H | H⋯A | D⋯A | D—H⋯A |
|---|---|---|---|---|
| N2—H23⋯O12S | 0.91 | 2.20 | 2.928 (15) | 136 |
| N3—H31⋯O17S | 0.91 | 2.32 | 3.032 (15) | 136 |
| O14—H14B⋯O25S | 0.85 (10) | 2.01 (9) | 2.754 (15) | 145 (6) |
| O5—H5A⋯O3Si | 0.86 (4) | 2.00 (4) | 2.809 (10) | 156 (3) |
| O4—H4B⋯O9Si | 0.85 (5) | 2.37 (6) | 3.05 (2) | 137 (3) |
| N2—H22⋯O4Sii | 0.91 | 2.23 | 3.022 (12) | 145 |
| N2—H21⋯O15Sii | 0.91 | 2.11 | 2.768 (19) | 129 |
| N1—H13⋯O16Sii | 0.91 | 2.02 | 2.906 (13) | 163 |
| N2—H22⋯O2Sii | 0.91 | 2.22 | 3.016 (12) | 147 |
| N4—H42⋯O7SBiii | 0.91 | 2.10 | 2.98 (5) | 163 |
| N3—H33⋯O22Siii | 0.91 | 1.94 | 2.822 (19) | 164 |
| N4—H41⋯O24Siii | 0.91 | 2.18 | 3.033 (12) | 156 |
| N4—H42⋯O5Siii | 0.91 | 2.31 | 3.049 (13) | 139 |
| N1—H11⋯O6Siv | 0.91 | 2.20 | 3.002 (15) | 147 |
| O3—H3B⋯O6Siv | 0.85 (5) | 2.33 (7) | 3.149 (15) | 161 (4) |
| N1—H12⋯O4Sv | 0.91 | 2.09 | 2.981 (11) | 165 |
| N2—H21⋯O23Svi | 0.91 | 2.30 | 2.924 (10) | 125 |
| O3—H3A⋯O23Svi | 0.85 (6) | 2.04 (5) | 2.882 (10) | 171 (4) |
| O4—H4A⋯O20Svi | 0.86 (6) | 2.01 (4) | 2.826 (10) | 158 (5) |
| N4—H43⋯O19Svii | 0.91 | 2.16 | 3.017 (11) | 156 |
| O16—H16B⋯O20Svii | 0.84 (10) | 2.16 (5) | 2.794 (11) | 133 (4) |
| N3—H32⋯O5Sviii | 0.91 | 2.06 | 2.926 (12) | 159 |
| O13—H13A⋯O8ix | 0.86 (3) | 2.01 (3) | 2.863 (10) | 174 (5) |
Symmetry codes: (i)
; (ii)
; (iii)
; (iv)
; (v)
; (vi)
; (vii)
; (viii)
; (ix)
.