| Bruker SMART CCD area-detector diffractometer | 2045 independent reflections |
| Radiation source: fine-focus sealed tube | 1676 reflections with I > 2σ(I) |
| graphite | Rint = 0.031 |
| φ and ω scans | θmax = 26.0°, θmin = 2.6° |
| Absorption correction: multi-scan (SADABS; Sheldrick, 1996) | h = −9→9 |
| Tmin = 0.959, Tmax = 0.994 | k = −11→12 |
| 6834 measured reflections | l = −16→15 |
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