Table 1. Hydrogen-bond geometry (Å, °).
| D—H⋯A | D—H | H⋯A | D⋯A | D—H⋯A |
|---|---|---|---|---|
| N1—H11N⋯O1i | 0.83 (2) | 2.28 (2) | 3.0527 (16) | 154 (2) |
| N1—H12N⋯O16 | 0.77 (2) | 2.38 (2) | 3.0647 (18) | 149 (2) |
| N2—H21N⋯O7i | 0.86 (2) | 2.01 (2) | 2.8245 (17) | 159 (2) |
| N2—H22N⋯O10 | 0.80 (2) | 2.53 (2) | 2.9844 (17) | 117.7 (19) |
| O2—H2O⋯O6ii | 0.77 (2) | 1.79 (2) | 2.5582 (15) | 174 (3) |
| O4—H4O⋯O11iii | 0.73 (3) | 1.94 (3) | 2.6593 (16) | 170 (3) |
| O13—H133⋯O5 | 1.06 (2) | 1.40 (3) | 2.4558 (16) | 174 (2) |
| O8—H8O⋯O15 | 0.81 (2) | 1.76 (2) | 2.5607 (17) | 173 (3) |
| O10—H10O⋯O16iv | 0.83 (3) | 1.80 (3) | 2.6298 (17) | 172 (3) |
| O12—H12O⋯O14 | 0.79 (2) | 1.71 (2) | 2.4608 (16) | 159 (3) |
| O13—H131⋯O3v | 0.80 (3) | 1.79 (3) | 2.5728 (16) | 165 (2) |
| O13—H132⋯O9vi | 0.89 (2) | 1.62 (2) | 2.5044 (16) | 174 (2) |
| O14—H141⋯O3vii | 0.79 (2) | 1.96 (2) | 2.7220 (16) | 162 (2) |
| O14—H142⋯O11viii | 0.80 (3) | 1.90 (3) | 2.6911 (17) | 171 (3) |
| O15—H151⋯O4ix | 0.82 (3) | 2.18 (3) | 2.9904 (18) | 169 (3) |
| O15—H152⋯O6iv | 0.79 (2) | 1.97 (2) | 2.7504 (17) | 176 (3) |
| O16—H161⋯O14ix | 0.76 (3) | 2.19 (3) | 2.8534 (16) | 147 (3) |
| O16—H162⋯O8x | 0.87 (3) | 2.48 (3) | 3.0109 (17) | 120 (2) |
| O16—H162⋯O2 | 0.87 (3) | 2.62 (3) | 3.1809 (16) | 123 (2) |
Symmetry codes: (i)
; (ii)
; (iii)
; (iv)
; (v)
; (vi)
; (vii)
; (viii)
; (ix)
; (x)
.