| Refinement on F2 | Primary atom site location: structure-invariant direct methods |
| Least-squares matrix: full | Secondary atom site location: difference Fourier map |
| R[F2 > 2σ(F2)] = 0.036 | Hydrogen site location: inferred from neighbouring sites |
| wR(F2) = 0.116 | H-atom parameters constrained |
| S = 1.01 | w = 1/[σ2(Fo2) + (0.0643P)2 + 1.1088P] where P = (Fo2 + 2Fc2)/3 |
| 4146 reflections | (Δ/σ)max = 0.001 |
| 298 parameters | Δρmax = 0.39 e Å−3 |
| 0 restraints | Δρmin = −0.26 e Å−3 |