Oxford Xcalibur Eos (Nova) CCD detector diffractometer | 1692 independent reflections |
Radiation source: Enhance (Mo) X-ray Source | 1176 reflections with I > 2σ(I) |
graphite | Rint = 0.034 |
ω scans | θmax = 25.5°, θmin = 2.8° |
Absorption correction: multi-scan (CrysAlis PRO RED; Oxford Diffraction, 2009) | h = −9→9 |
Tmin = 0.916, Tmax = 0.987 | k = −9→10 |
7291 measured reflections | l = −17→17 |