Goniometer Xcalibur diffractometer with a Ruby (Gemini Cu) detector | 3123 independent reflections |
Radiation source: Enhance (Cu) X-ray Source | 2731 reflections with I > 2σ(I) |
graphite | Rint = 0.025 |
Detector resolution: 10.5081 pixels mm-1 | θmax = 74.2°, θmin = 4.8° |
ω scans | h = −8→5 |
Absorption correction: multi-scan (CrysAlis RED; Oxford Diffraction, 2007) | k = −10→11 |
Tmin = 0.200, Tmax = 0.557 | l = −15→16 |
5138 measured reflections |