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. 2009 Dec 16;66(Pt 1):o163–o164. doi: 10.1107/S1600536809053410
Goniometer Xcalibur diffractometer with a Ruby (Gemini Cu) detector 3123 independent reflections
Radiation source: Enhance (Cu) X-ray Source 2731 reflections with I > 2σ(I)
graphite Rint = 0.025
Detector resolution: 10.5081 pixels mm-1 θmax = 74.2°, θmin = 4.8°
ω scans h = −8→5
Absorption correction: multi-scan (CrysAlis RED; Oxford Diffraction, 2007) k = −10→11
Tmin = 0.200, Tmax = 0.557 l = −15→16
5138 measured reflections