Rigaku AFC12K/SATURN724 diffractometer | 3072 independent reflections |
Radiation source: fine-focus sealed tube | 3020 reflections with I > 2σ(I) |
graphite | Rint = 0.089 |
ω scans | θmax = 26.5°, θmin = 4.0° |
Absorption correction: multi-scan (ABSCOR; Higashi, 1995) | h = −9→8 |
Tmin = 0.884, Tmax = 1 | k = −13→14 |
13441 measured reflections | l = −21→20 |