Table 2.
| ||||||
---|---|---|---|---|---|---|
entry | R | Ar | R1 | yield (%)b | ||
1 | Ph | Ph | Ph | 63 (5) | ||
2 | 3-OMe-Ph | Ph | Ph | 60 (6) | ||
3 | 2-OMe-Ph | Ph | Ph | 66 (7) | ||
4 | 2-Naphthyl | Ph | Ph | 64 (8) | ||
5 | 4-Cl-Ph | Ph | Ph | 61 (9) | ||
6 | 2-OMe-Ph | Ph | 3-Me-Ph | 64 (10) | ||
7 | Me | Ph | 2-Me-Ph | 82 (11) | ||
8 | CH2CH2CH3 | Ph | 3-Me-Ph | 84 (12) | ||
9 | Ph | Ph | 4-Cl-Ph | 68 (13) | ||
10 | Ph | Ph | 4-F-Ph | 61 (14) | ||
11 | Ph | Ph | 3-Me-Ph | 73 (15) | ||
12 | Ph | 3-Me-Ph | Ph | 71 (16) | ||
13 | Ph | 4-Me-Ph | Ph | 63 (17) |
3 equiv of 2.
Isolated yields after chromatography.