| Rigaku R-AXIS RAPID diffractometer | 4457 independent reflections |
| Radiation source: rolling anode | 3114 reflections with I > 2σ(I) |
| graphite | Rint = 0.021 |
| Detector resolution: 10.00 pixels mm-1 | θmax = 27.4°, θmin = 3.0° |
| ω scans | h = −11→11 |
| Absorption correction: multi-scan (ABSCOR; Higashi, 1995) | k = −13→13 |
| Tmin = 0.931, Tmax = 0.963 | l = −13→13 |
| 9742 measured reflections |
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