Rigaku Saturn724 CCD camera diffractometer | 2284 independent reflections |
Radiation source: rotating anode | 2003 reflections with I > 2σ(I) |
multilayer | Rint = 0.051 |
ω scans | θmax = 26.0°, θmin = 1.8° |
Absorption correction: multi-scan (CrystalClear-SM Expert; Rigaku, 2009) | h = −13→13 |
Tmin = 0.989, Tmax = 0.996 | k = −8→8 |
10183 measured reflections | l = −17→15 |