| Bruker SMART APEX CCD area-detector diffractometer | 1420 independent reflections |
| Radiation source: fine-focus sealed tube | 1328 reflections with I > 2σ(I) |
| graphite | Rint = 0.049 |
| phi and ω scans | θmax = 25.0°, θmin = 2.1° |
| Absorption correction: multi-scan (SADABS; Bruker, 2000) | h = −8→8 |
| Tmin = 0.751, Tmax = 0.761 | k = −14→14 |
| 10614 measured reflections | l = −23→23 |
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