Refinement on F2	Primary atom site location: structure-invariant direct methods
Least-squares matrix: full	Secondary atom site location: difference Fourier map
R[F2 > 2σ(F2)] = 0.051	Hydrogen site location: difference Fourier map
wR(F2) = 0.167	H atoms treated by a mixture of independent and constrained refinement
S = 1.14	w = 1/[σ2(Fo2) + (0.0959P)2] where P = (Fo2 + 2Fc2)/3
14856 reflections	(Δ/σ)max = 0.006
787 parameters	Δρmax = 1.40 e Å−3
12 restraints	Δρmin = −1.14 e Å−3