Oxford Diffraction Xcalibur Sapphire 3 diffractometer	7060 independent reflections
Radiation source: fine-focus sealed tube	5177 reflections with I > 2σ(I)
graphite	Rint = 0.020
Detector resolution: 16.0855 pixels mm-1	θmax = 72.6°, θmin = 4.6°
ω scans	h = −14→11
Absorption correction: multi-scan (CrysAlis RED; Oxford Diffraction, 2009)	k = −15→15
Tmin = 0.947, Tmax = 1.000	l = −16→16
11434 measured reflections