| Bruker SMART APEX diffractometer | 1338 reflections with I > 2σ(I) |
| Radiation source: fine-focus sealed tube | Rint = 0.040 |
| graphite | θmax = 27.5°, θmin = 1.8° |
| ω scans | h = −7→7 |
| 6694 measured reflections | k = −11→13 |
| 1699 independent reflections | l = −14→14 |
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