| Br1—C1 | 1.9624 (14) | C3—H3B | 0.990 |
| Br2—C1 | 1.9250 (14) | C3—C4 | 1.527 (2) |
| O1—H1O | 0.83 (3) | C4—H4A | 0.990 |
| O1—C2 | 1.3949 (17) | C4—H4B | 0.990 |
| O2—C5 | 1.2286 (18) | C6—H6 | 0.97 (2) |
| O3—C5 | 1.3360 (17) | C6—C7 | 1.513 (2) |
| O3—C6 | 1.4641 (18) | C6—C8 | 1.510 (2) |
| N—C2 | 1.4457 (18) | C7—H7A | 0.980 |
| N—C3 | 1.4695 (19) | C7—H7B | 0.980 |
| N—C5 | 1.3478 (19) | C7—H7C | 0.980 |
| C1—C2 | 1.546 (2) | C8—H8A | 0.980 |
| C1—C4 | 1.517 (2) | C8—H8B | 0.980 |
| C2—H2 | 1.000 | C8—H8C | 0.980 |
| C3—H3A | 0.990 | ||
| H1O—O1—C2 | 106.6 (19) | C1—C4—H4B | 111.3 |
| C5—O3—C6 | 117.15 (11) | C3—C4—H4A | 111.3 |
| C2—N—C3 | 114.36 (12) | C3—C4—H4B | 111.3 |
| C2—N—C5 | 121.99 (12) | H4A—C4—H4B | 109.2 |
| C3—N—C5 | 123.58 (12) | O2—C5—O3 | 124.43 (13) |
| Br1—C1—Br2 | 108.05 (7) | O2—C5—N | 124.50 (13) |
| Br1—C1—C2 | 107.27 (9) | O3—C5—N | 111.06 (12) |
| Br1—C1—C4 | 110.95 (9) | O3—C6—H6 | 107.0 (13) |
| Br2—C1—C2 | 113.74 (9) | O3—C6—C7 | 105.83 (12) |
| Br2—C1—C4 | 112.98 (10) | O3—C6—C8 | 109.23 (12) |
| C2—C1—C4 | 103.71 (12) | H6—C6—C7 | 111.1 (13) |
| O1—C2—N | 110.45 (12) | H6—C6—C8 | 110.8 (13) |
| O1—C2—C1 | 111.97 (11) | C7—C6—C8 | 112.58 (13) |
| O1—C2—H2 | 111.3 | C6—C7—H7A | 109.5 |
| N—C2—C1 | 99.99 (11) | C6—C7—H7B | 109.5 |
| N—C2—H2 | 111.3 | C6—C7—H7C | 109.5 |
| C1—C2—H2 | 111.3 | H7A—C7—H7B | 109.5 |
| N—C3—H3A | 111.3 | H7A—C7—H7C | 109.5 |
| N—C3—H3B | 111.3 | H7B—C7—H7C | 109.5 |
| N—C3—C4 | 102.54 (11) | C6—C8—H8A | 109.5 |
| H3A—C3—H3B | 109.2 | C6—C8—H8B | 109.5 |
| H3A—C3—C4 | 111.3 | C6—C8—H8C | 109.5 |
| H3B—C3—C4 | 111.3 | H8A—C8—H8B | 109.5 |
| C1—C4—C3 | 102.32 (11) | H8A—C8—H8C | 109.5 |
| C1—C4—H4A | 111.3 | H8B—C8—H8C | 109.5 |
| C3—N—C2—O1 | 99.81 (14) | Br1—C1—C4—C3 | 73.49 (12) |
| C3—N—C2—C1 | −18.30 (15) | Br2—C1—C4—C3 | −165.00 (10) |
| C5—N—C2—O1 | −77.31 (17) | C2—C1—C4—C3 | −41.39 (13) |
| C5—N—C2—C1 | 164.59 (13) | N—C3—C4—C1 | 29.33 (14) |
| Br1—C1—C2—O1 | 161.81 (9) | C6—O3—C5—O2 | 5.0 (2) |
| Br1—C1—C2—N | −81.21 (11) | C6—O3—C5—N | −176.05 (12) |
| Br2—C1—C2—O1 | 42.39 (14) | C2—N—C5—O2 | 0.1 (2) |
| Br2—C1—C2—N | 159.37 (9) | C2—N—C5—O3 | −178.85 (12) |
| C4—C1—C2—O1 | −80.72 (13) | C3—N—C5—O2 | −176.76 (14) |
| C4—C1—C2—N | 36.26 (13) | C3—N—C5—O3 | 4.3 (2) |
| C2—N—C3—C4 | −6.68 (16) | C5—O3—C6—C7 | 152.87 (13) |
| C5—N—C3—C4 | 170.38 (13) | C5—O3—C6—C8 | −85.69 (15) |