| Bruker APEXII area-detector diffractometer | 3792 independent reflections |
| Radiation source: fine-focus sealed tube | 2335 reflections with I > 2σ(I) |
| graphite | Rint = 0.025 |
| φ and ω scans | θmax = 27.3°, θmin = 2.2° |
| Absorption correction: multi-scan (SADABS; Bruker, 2004) | h = −8→6 |
| Tmin = 0.977, Tmax = 0.983 | k = −12→14 |
| 5311 measured reflections | l = −16→16 |