Bruker X8 APEXII diffractometer | 3393 independent reflections |
Radiation source: fine-focus sealed tube | 2577 reflections with I > 2σ(I) |
graphite | Rint = 0.040 |
φ and ω scans | θmax = 29.7°, θmin = 2.7° |
Absorption correction: multi-scan (SADABS; Sheldrick, 1996) | h = −13→13 |
Tmin = 0.256, Tmax = 0.428 | k = −12→12 |
51411 measured reflections | l = −18→18 |